{"id":1090201,"date":"2025-09-04T10:31:30","date_gmt":"2025-09-04T08:31:30","guid":{"rendered":"https:\/\/plastanalisi.com\/?p=1090201"},"modified":"2025-09-04T10:50:07","modified_gmt":"2025-09-04T08:50:07","slug":"identificazione-additivo-lubrificante-in-campione-pom","status":"publish","type":"post","link":"https:\/\/plastanalisi.com\/it\/case-study\/2025\/identificazione-additivo-lubrificante-in-campione-pom\/","title":{"rendered":"Identificazione di Additivo Lubrificante in un Campione in POM"},"content":{"rendered":"

[et_pb_section fb_built=”1″ _builder_version=”4.27.4″ _module_preset=”default” global_colors_info=”{}” theme_builder_area=”post_content”][et_pb_row _builder_version=”4.27.4″ _module_preset=”default” global_colors_info=”{}” theme_builder_area=”post_content”][et_pb_column type=”4_4″ _builder_version=”4.27.4″ _module_preset=”default” global_colors_info=”{}” theme_builder_area=”post_content”][et_pb_image src=”https:\/\/plastanalisi.com\/wp-content\/uploads\/2025\/09\/bushing-white-1.png” alt=”white bushing ” title_text=”white bushing ” _builder_version=”4.27.4″ _module_preset=”default” width=”51%” global_colors_info=”{}” theme_builder_area=”post_content”][\/et_pb_image][et_pb_text _builder_version=”4.27.4″ _module_preset=”default” hover_enabled=”0″ global_colors_info=”{}” theme_builder_area=”post_content” sticky_enabled=”0″]<\/p>\n

Cosa chiede il cliente<\/h4>\n

Un nostro cliente si \u00e8 rivolto a noi con una richiesta specifica: identificare la presenza e la percentuale di un additivo lubrificante in un campione polimerico in Poliossimetilene (POM).<\/strong> L’obiettivo era chiaro: capire quale fosse l’agente lubrificante utilizzato e in che quantit\u00e0, un’informazione fondamentale per ottimizzare le propriet\u00e0 tribologiche del materiale, come la riduzione dell’attrito e dell’usura.
Gli additivi lubrificanti, come il PTFE, il bisolfuro di molibdeno (MoS2), la grafite o i siliconi, sono spesso aggiunti ai polimeri durante la fase di compounding per migliorarne le prestazioni. Il loro meccanismo d’azione pu\u00f2 variare: alcuni formano una pellicola superficiale, altri si diffondono lentamente dal nucleo del materiale, e altri ancora, come le cariche a struttura lamellare, riducono gli sforzi di taglio.<\/p>\n

La soluzione proposta da Plastanalisi<\/h4>\n

Dopo un’attenta valutazione, abbiamo proposto una strategia di analisi combinata, basandoci sulla nostra esperienza pluriennale nel campo delle analisi sui polimeri. Dato che il campione si presentava di colore bianco, abbiamo subito ristretto il campo della ricerca ai lubrificanti pi\u00f9 probabili: il PTFE e il silicone.<\/p>\n

Per il PTFE, abbiamo utilizzato una combinazione di tecniche: l’analisi termica DSC<\/strong> per la verifica qualitativa (presenza\/assenza) e la cromatografia ionica (IC)<\/strong> per la quantificazione precisa. Parallelamente, per il silicone, abbiamo proceduto con un’estrazione mirata del materiale, seguita da un’analisi FT-IR<\/strong> (Spettroscopia a infrarossi in trasformata di Fourier) per confermarne la presenza e, infine, determinarne la percentuale in peso.<\/p>\n

Risultati analisi<\/h4>\n

Le nostre analisi hanno portato a un risultato chiaro. Abbiamo riscontrato la presenza di un solo additivo lubrificante all’interno del campione: silicone, con un contenuto in peso pari al 2%. La spettroscopia FT-IR ha confermato la struttura chimica del silicone, fornendo una prova inconfutabile.
Questo dato ha fornito al cliente un’informazione preziosa per il suo progetto. Il successo di questa indagine dimostra l’efficacia delle nostre metodologie e la capacit\u00e0 del nostro laboratorio di risolvere sfide complesse, fornendo risposte concrete e affidabili.<\/p>\n

Presenza di additivo lubrificante di natura siliconica : 2% in peso.<\/strong><\/p>\n

<\/strong><\/p>\n

\"identification<\/strong><\/p>\n

 <\/p>\n

[\/et_pb_text][\/et_pb_column][\/et_pb_row][\/et_pb_section]<\/p>\n","protected":false},"excerpt":{"rendered":"

Cosa chiede il cliente Un nostro cliente si \u00e8 rivolto a noi con una richiesta specifica: identificare la presenza e la percentuale di un additivo lubrificante in un campione polimerico in Poliossimetilene (POM). L’obiettivo era chiaro: capire quale fosse l’agente lubrificante utilizzato e in che quantit\u00e0, un’informazione fondamentale per ottimizzare le propriet\u00e0 tribologiche del materiale, […]<\/p>\n","protected":false},"author":1,"featured_media":1090192,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_et_pb_use_builder":"on","_et_pb_old_content":"[et_pb_section fb_built=\"1\" _builder_version=\"4.27.4\" _module_preset=\"default\" global_colors_info=\"{}\" theme_builder_area=\"et_body_layout\"][et_pb_row _builder_version=\"4.27.4\" _module_preset=\"default\" global_colors_info=\"{}\" theme_builder_area=\"et_body_layout\"][et_pb_column type=\"4_4\" _builder_version=\"4.27.4\" _module_preset=\"default\" global_colors_info=\"{}\" theme_builder_area=\"et_body_layout\"][et_pb_image src=\"https:\/\/plastanalisi.com\/wp-content\/uploads\/2025\/09\/bushing-white-1.png\" alt=\"white bushing \" title_text=\"white bushing \" _builder_version=\"4.27.4\" _module_preset=\"default\" width=\"51%\" hover_enabled=\"0\" global_colors_info=\"{}\" theme_builder_area=\"et_body_layout\" sticky_enabled=\"0\"][\/et_pb_image][et_pb_text _builder_version=\"4.27.4\" _module_preset=\"default\" hover_enabled=\"0\" global_colors_info=\"{}\" theme_builder_area=\"et_body_layout\" sticky_enabled=\"0\"]\n

Client request<\/h4>\n

A client came to us with a specific request: to identify the presence and percentage of a lubricant additive in a polyoxymethylene (POM) polymer sample.<\/strong> The goal was clear: to understand which lubricant agent was used and in what quantity. This information is crucial for optimizing the material's tribological properties, such as reducing friction and wear.\nLubricant additives like PTFE, molybdenum disulfide (MoS2), graphite, or silicones are often added to polymers during the compounding phase to improve their performance. Their mechanism of action can vary: some form a surface film, others slowly diffuse from the core of the material, and still others, such as those with a lamellar structure, reduce shear stress.<\/p>\n\n

The solution proposed by Plastanalisi<\/h4>\n

After a careful evaluation, we proposed a combined analysis strategy based on our many years of experience in polymer analysis. Since the sample was white, we immediately narrowed the search to the most likely lubricants: PTFE and silicone.\nFor the PTFE, we used a combination of techniques: DSC thermal analysis<\/strong> for qualitative verification (presence\/absence) and ion chromatography (IC)<\/strong> for precise quantification. Simultaneously, for the silicone, we performed a targeted extraction of the material, followed by an FT-IR analysis<\/strong> (Fourier-transform infrared spectroscopy) to confirm its presence and, finally, determine its percentage by weight.<\/p>\n\n

Analysis results<\/h4>\n

Our analysis led to a clear result. We found only one lubricant additive inside the sample: silicone, with a content of 2% by weight. The FT-IR spectroscopy confirmed the chemical structure of the silicone, providing irrefutable proof.\nThis data provided the client with valuable information for their project. The success of this investigation demonstrates the effectiveness of our methodologies and our laboratory's ability to solve complex challenges, providing concrete and reliable answers.\nPresence of a silicone-based lubricant additive: 2% by weight<\/strong><\/p>\n

\"identification<\/strong><\/p>\n \n\n[\/et_pb_text][\/et_pb_column][\/et_pb_row][\/et_pb_section]","_et_gb_content_width":"","footnotes":""},"categories":[10],"tags":[],"class_list":["post-1090201","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-case-study"],"yoast_head":"\nIdentificazione di Additivo Lubrificante in un Campione in POM | Plastanalisi<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/plastanalisi.com\/it\/case-study\/2025\/identificazione-additivo-lubrificante-in-campione-pom\/\" \/>\n<meta property=\"og:locale\" content=\"it_IT\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Identificazione di Additivo Lubrificante in un Campione in POM | Plastanalisi\" \/>\n<meta property=\"og:description\" content=\"Cosa chiede il cliente Un nostro cliente si \u00e8 rivolto a noi con una richiesta specifica: identificare la presenza e la percentuale di un additivo lubrificante in un campione polimerico in Poliossimetilene (POM). 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